Elettra
BL 07.1 - MCX

Welcome to the MCX beamline!

The Materials Characterisation by X-ray diffraction (MCX) beamline allows to perform a wide range of non-single crystal diffraction experiments: grazing angle diffraction and reflectivity, residual stress and texture analysis, phase identification and structural studies. Systems that can be investigated vary from organic and inorganic thin films, to thermally and/or mechanically modified surfaces of mechanic components, to polymers, catalysts and highly disordered materials in the form of films, powders, fibers. In addition to studies in the fields of the scientific heritage and earth sciences, a valuable activity is the characterization of new electrode materials by operando measurements on batteries.

Beamline Energy Range
6 - 20 [keV]
Max Flux On Sample
10 * 1011 [ph/s] @ 9 [keV]
Spot Size On Sample Hor
300 - 2000 [um]
Spot Size On Sample Vert
300 - 1000 [um]
Divergence Hor
0.1 - 1 [urad]
Divergence Vert
0.05 - 0.3 [urad]
Photon Sources

Bending magnet 2.0

Type
Bending Magnet
Source Size Sigma
X = 139 [um], Y = 28 [um]

Bending magnet 2.4

Type
Bending Magnet
Source Size Sigma
X = 197 [um], Y = 30 [um]
Monochromators

Monochromator

Energy Range
6 - 20 [keV]
Type
Crystal monochromator: Si 111
Pre-focusing Mirror Type
cilndrical
Refocusing Mirror Type
cilindrical
Endstations or Setup

Diffractometer

Description
4 circle diffractometer with xyz translation stage. Other availble equipment for this set-up ; Gasblower (max 1000°C), Cryojet (Min.100K), cooling/heating chamber (Min -20°C - Max 130°C)
Diffractometer
Huber 4-circle diffractometer with 3D translation stage
Detectors Available
fast scintillator detector
Silicon Drift Detector
marCCD
Endstation Operative
Yes

Sample

Sample Type
Powder
Other Sample Type
Thin films and any other polycristalline objects

Manipulator or Sample stage

Positioning Precision
X = 1 [um], Y = 1 [um], Z = 1 [um]
Range Of Movement
X = 15 [mm], Y = 15 [mm], Z = 5 [mm]

Sample Holders

Type
Flat plate spinner
Type
Capillary spinner

Furnace

Description
Furnace with an atmosphere and temperature controlled environment for powders in capillaries. The diffraction patterns are collected on a translating image plate (IP).
Diffractometer
Furnace maximum temperature 1000°C.
Endstation Operative
Yes

Sample

Sample Type
Powder
Mounting Type
capillary (optional with controlled gas-flow )

Manipulator or Sample stage

Sample Environment

Temperature
300 - 1273 [K]

Sample Holders

Type
Capillary spinner
Detectors

fast scintillator detector

Type
Fast scintillator counter
Passive or Active (Electronics)
Active
Dynamic Range
3 * 105 [counts/s]

Detection

Detected Particle
Photon

marCCD

Type
marCCD-SX-165
Pixel Size
X = 80 [um], Y = 80 [um]
Array Size
X = 2048 [pixel], Y = 2048 [pixel]
Passive or Active (Electronics)
Active
Dynamic Range
16 [bits]

Detection

Detected Particle
Photon

Silicon Drift Detector

Type
Silicon Drift Detector
Passive or Active (Electronics)
Active

Detection

Detected Particle
Photon
contacts
Jasper PLAISIER
Lara GIGLI
Techniques
Diffraction
  • Crystallography
  • Powder diffraction
Emission or Reflection
  • Reflectrometry
  • X-ray fluorescence (XRF)
Disciplines
Chemistry
  • Catalysis
  • Green Chemistry
  • Physical Chemistry
Earth Sciences & Environment
  • Geology
  • Other - Earth Sciences & Environment
Energy
  • Other - Energy
  • Sustainable energy systems
Engineering & Technology
  • Aeronautics
  • Nanotechnology & production processes
  • Space
Humanities
  • Cultural Heritage
Life Sciences & Biotech
  • Medicine
Material Sciences
  • Knowledge based multifunctional materials
  • Other - Material Sciences
Physics
  • Hard condensed matter - structures
  • Surfaces, interfaces and thin films
Address
MCX - Elettra-Sincrotrone Trieste S.C.p.A.
Strada Statale 14 - km 163,5 in AREA Science Park
34149 Basovizza, Trieste ITALY
control/Data analysis
Control Software Type
  • In house developed software written in Python/PyQt
Data Output Type
  • 1D and 2D Diffraction patterns
Data Output Format
  • ascii (xy, gsas), tiff
Softwares For Data Analysis
  • PDF4, GSAS, FullProf, Elin
Equipment That Can Be Brought By The User
Any. Please contact the beamline staff